Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the. Copper – Copper Sulfate – 16% sulfuric acid, ASTM A – Practice E (Strauss Test) This procedure is conducted to determine the susceptibility of austenitic. ASTM A Practice E test. This practice describes the procedure by which the copper-copper sulfate% sulfuric acid test is conducted to determine .
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Some specific hazards statements are given in Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
Discover perspectives, resources, s advice from our world-leading Engaged Experts. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.
At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. Because it can be run quickly for screening, we often run this test first.
How do you select the right ASTM corrosion testing method for your material? In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. If the structure is acceptable no additional testing is required. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
This method is a hour boiling test for “as received” specimens of stainless asm. Classification of the structure after A W262 A analysis will determine if the material is acceptable or if additional testing is required.
The test evaluates the resistance of extra-low-carbon steels to practive and intergranular attack from welding or heat treatment processes.
Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 prractice.
This abstract is a brief summary of the referenced ast. In everyday applications, corrosion varies by materials and solutions.
Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack. Wilson Hardness Conversion Chart. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.
Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. If you are not sure, please contact us for assistance.
ASTM A Intergranular Corrosion Testing and Analysis
Contact us now for pricing or a quote! All austenitic stainless steels should meet this requirement, if proper annealing took place. Please refer to practide specification for more details.
Carbon and Sulfur Analysis. This method is preferable for chromium depletions and corrosion in intermetallic phases. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. These practices include five intergranular corrosion tests, namely: It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. These tests are often run as a qualification test to ensure each batch of stainless pracice is properly prepared.
The level of corrosion is determined by mass loss. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. This practice includes boiling the sample for 24 adtm hours in the solution above, and measures the materials performance quantitatively.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Please share this page: This practicr is for detecting susceptibility to intergranular attack IGA. Link to Active This link will always route to the current Active version of the standard. This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.
The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack.
Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. The Copper Sulfate Test is especially effective for determining ppractice to intergranular attack for low carbon steels. There ast several cause for SCC, Chloride is the leading cause of transgranular cracking or attack.
Share on Tumblr Print. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
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